Synthesis of nickel–zinc ferrite nanoparticles in polyol: morphological, structural and magnetic studies
Identifieur interne : 000195 ( France/Analysis ); précédent : 000194; suivant : 000196Synthesis of nickel–zinc ferrite nanoparticles in polyol: morphological, structural and magnetic studies
Auteurs : Z. Beji [Tunisie, France] ; T. Ben Chaabane [Tunisie] ; L. S. Smiri [Tunisie] ; S. Ammar [France] ; F. Fiévet [France] ; N. Jouini [France] ; J. M. Grenèche [France]Source :
- physica status solidi (a) [ 1862-6300 ] ; 2006-02.
English descriptors
Abstract
Nickel–zinc ferrite monodisperse nanoparticles are synthesized by forced hydrolysis in diethylenglycol. FC and ZFC susceptibility curves suggest that they present superparmagnetic behaviour with a blocking temperature between 63 and 15 K depending on the zinc content. The saturation magnetization of the nanocrystals at 5 K is very close to that of bulk materials, and very high compared to that of similar particles prepared by other chemical routes. High Resolution Transmission Electron Microscopy and In‐field Mössbauer studies show clearly that these relatively high values are mainly due to: (i) the high crystalline quality of the particles and (ii) a cation distribution different from the classical distribution encountered in the bulk material. (© 2006 WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim)
Url:
DOI: 10.1002/pssa.200521454
Affiliations:
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ISTEX:B7A66A2146CBB58FAF27453FD10C1D4AE067B4F0Le document en format XML
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FC and ZFC susceptibility curves suggest that they present superparmagnetic behaviour with a blocking temperature between 63 and 15 K depending on the zinc content. The saturation magnetization of the nanocrystals at 5 K is very close to that of bulk materials, and very high compared to that of similar particles prepared by other chemical routes. High Resolution Transmission Electron Microscopy and In‐field Mössbauer studies show clearly that these relatively high values are mainly due to: (i) the high crystalline quality of the particles and (ii) a cation distribution different from the classical distribution encountered in the bulk material. (© 2006 WILEY‐VCH Verlag GmbH & Co. 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